To access NMR data for Dr. Nalli's Chemistry 351 labs:
1. From a PC, click START, choose RUN enter STORECLASSES and click OK
2. Enter your username and password.
- Explore our latest ECZ series of NMR Spectrometers. Over 60 years of expertise offering world class NMRs, starting in 1956 with the first NMR from JEOL.
- Ref Code: DWG-NMR-001 Issue No. 001 Page: 3/24 1 Aim The aim of this practical guideline is to support the forensic community with special knowledge on quantitative Nuclear Magnetic Resonance(qNMR) analysis. QNMR has special requirements in comparison to chromatographic methods. The method is very.
3. Scroll down to the folder 20115000599M
614 CHAPTER 13. NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY In many spectra, geminal, four-bond, and five-bond splittings are not readily discernible as clearly separated lines, but instead are manifested as perceptibly broadened peaks. Such is the case, for example, in the NMR spectrum in Fig. 13.16 (Problem 13.24). Free download delta programming language Files at Software Informer. The Gentee programming language can be classified as a procedure-oriented language with some features typical of object-oriented.
4. The data you need will be in the read-only subfolder. You should copy all needed files to your machine for guaranteed easy access later.
5. I recommend that you create a shortcut to this folder by right clicking on it and selecting 'send to Desktop (create shortcut)'. Now you will have easy access to it in the future.
To install Delta (software for processing NMR files).
- For PCs running Windows XP. Go to start menu and choose 'Run'. Use copy and paste to enter appsrv1appsInstallspcChemistry in the dialog box that opens. Then double click the Install_Delta_XP_ONLY file. Be sure to select 'Minimal' rather than 'Typical' as the installation option.
- For PCs running Windows 7 or Vista: You must be on campus connected via your wired network connection. Make sure wireless is turned off during the install. 2.) Go to Start => Run 3.) Enter: appsrv1appsInstallspcChemistryDataDelta and click OK 4.) Copy the file DeltaInstaller_v4.3.6.exe to your desktop. 5.) From the desktop, Right click on the DeltaInstaller_4.3.6.exe file and select properties. 6.) Click on the Compatibility tab. 7.) Check on 'Run this program in compatibility mode for:'. 8.) From the pull down menu select 'Windows XP (Service Pack 2)'. 9.) Click OK at the bottom of the Properties window. 10.) Double click the DeltaInstaller_4.3.6.exe file to start the install process. Delta v4.3.6 should now install without problems. Be sure to select 'Minimal' rather than 'Typical' as the installation option. If it asks if you want to install for spectrometer control, press CANCEL.
- For Macs: You must be on campus connected via your wired network connection. Make sure wireless is turned off during the install. 1.) Click Go -> Connect to Server 2.) Type: smb://appsrv1.winona.edu/apps/installs/pc/Chemistry/Mac and click Connect 3.) Drag the DeltaInstaller file to your desktop 4.) Double click on the DeltaInstaller file on your desktop 5.) The installer will launch and warn that, 'You need an Administrator password to install the software' -Click on the lock icon and enter your password (same as your email password) Click OK 6.) Click Next 7.) Click 'I accept the terms of the License Agreement' 8.) Click Next 9.) Click Next 10.) Click Install -Click Cancel when it asks to Update Spectrometer -Click Done Delta will be installed to your Applications folder.
2. Once installed you will need to unlock the program by entering the license key, which is available at the course D2L site. Start the Delta program then select 'Installation' under the file menu and enter the license key there.
3. Start up the program and please make the following changes under 'Preferences' under the 'File' menu:
- Under the Printer tab set 'Print JEOL Logo' to FALSE, 'Parameters Location' to BOTTOM, and 'Plot Data Thickness' and 'Plot Integral Thickness' both to 0.10. (Note: Delta is unusual in that it requires you to keep the cursor in the box when you are changing parameters.)
- Under the Processors tab set 'Process 1D: Show FID' to FALSE. Click on 'Save & Close'
To process NMR files using Delta:.
Delta Nmr Software
- Basic instructions for using Delta were provided in Chem 350. Some of these instructions can be found within the linked documents for expts 2 and 3 from last semester. See http://course1.winona.edu/tnalli/f10/labsched.htm. There are many subtleties involved in processing a spectrum well, however, and I am always happy to help students process their NMR files during my office hours.
Delta Software For Nmr Chart
To up set up Delta so you can print directly to a networked printer:
- Open up Delta and select <File> <Preferences>
- Choose <Options> then <Printer Configure>
- In the 'title' box, type printsrv1.winona.eduslc386 (or at the end substitute the name of your favorite network printer instead of slc386)
- In the 'Printer' scroll box select the printer you just added and check that the 'B&W' button is depressed and the 'posterize' button is not selected. Click <save>.
- Now go to the Printer/Plotter tab (3rd from left) and click on <edit>. In the value box enter the full address of the printer again exactly as it was entered in step 3. Click <save and close> to exit out of the preferences menu.
- To print using a Mac note the following: When you attempt to primpt Delta sends the print job to the printer. However, for some reason the job is always on hold. Just manually open the printer job by going to System Preferences/Printer & Fax/ - Double click on the printer that the print job has been sent to. A new window with the name of the printer will open and show the job sent to the printer. Choose that job and hit ' Resume'. (You might be asked for your user name and password.)